Formation of Mn-doped iron silicides by ball milling View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2006-02

AUTHORS

J. Desimoni, S. M. Cotes, M. A. Taylor, R. C. Mercader

ABSTRACT

Using X-ray diffraction (XRD) and Mössbauer spectroscopy, we have studied the sequence of phase formations in the solid Mn-doped iron silicide series Fe1−xMnxSi2, with 0.00 ≤ x ≤ 0.12, in samples prepared by mechanical alloying from the pure elements. The milling was carried out at room temperature in Ar atmosphere in a horizontal mill for 15 h. The XRD patterns display broad lines, which can be ascribed to stable and metastable iron silicides like β-FeSi2, ɛ-FeSi, α-FeSi2, MnSi, and Si. The set of hyperfine parameters obtained support the coexistence of β-FeSi2, α-FeSi2 and ɛ-FeSi, in agreement with the XRD results. No replacement of Fe by Mn atoms in the regular sites of β-FeSi2 has been observed. More... »

PAGES

959-964

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Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10751-006-9396-0

DOI

http://dx.doi.org/10.1007/s10751-006-9396-0

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https://app.dimensions.ai/details/publication/pub.1038867692


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