Crystalsolvates of N-(3-ethylthio-1,2,4-thiadiazol-5-yl-aminocarbonylmethyl)cytisine View Full Text


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Article Info

DATE

2008-07

AUTHORS

U. S. Makhmudov, K. K. Turgunov, B. Tashkhodzhaev, V. A. Saprykina, Kh. M. Shakhidoyatov

ABSTRACT

The crystal structures of N-(3-ethylthio-1,2,4-thiadiazol-5-yl-aminocarbonylmethyl)cytisine with waters of hydration, water and methanol, and acetone were studied by x-ray diffraction. Three conformers formed by rotation of the 3-ethylthio-1,2,4-thiadiazol-5-yl-aminocarbonylmethyl moiety relative to the cytisine core were detected in the studied crystal structures. Different conformations of N-(3-ethylthio-1,2,4-thiadiazol-5-yl-aminocarbonylmethyl)cytisine and intermolecular H-bonds may have favored formation of different crystal solvates depending on the crystallization conditions. More... »

PAGES

466-471

References to SciGraph publications

  • 2008-06. Crystal solvates and polymorphs of N-(3-methylthio-1,2,4-thiadiazol-5-yl-aminocarbonylmethyl)cytisine in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/s10600-008-9098-8

    DOI

    http://dx.doi.org/10.1007/s10600-008-9098-8

    DIMENSIONS

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