Synthesis and properties of 3-azido-4-(2H-tetrazol-5-yl)furazan View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2017-06

AUTHORS

Andrei I. Stepanov, Vladimir S. Sannikov, Dmitry V. Dashko, Aleksey G. Roslyakov, Alexander A. Astrat’yev, Elena V. Stepanova, Zainutdin G. Aliev, Tel’man K. Goncharov, Sergei M. Aldoshin

ABSTRACT

We describe an effective scheme for the synthesis of a new energetic compound – 3-azido-4-(2H-tetrazol-5-yl)furazan from 4-amino-N'-hydroxyfurazan-3-carboximidamide. The structure of 3-azido-4-(2H-tetrazol-5-yl)furazan was proved by 1Н and 13С NMR spectroscopy, mass spectrometry, and X-ray structural analysis. 3-Azido-4-(2H-tetrazol-5-yl)furazan crystallized in monoclinic syngony, space group Р21/n, monocrystal density d 1.953 g·cm–3 (100 K). According to differential scanning calorimetry data, 3-azido-4-(2Htetrazol-5-yl)furazan melts at 103.3°С, while the maximum of thermal decomposition exotherm was observed at 185.6°С. The sensitivity of 3-azido-4-(2H-tetrazol-5-yl)furazan to impact (2 kg, 25 cm, 36% explosion frequency) and to friction (1450 kg·cm–3 lower limit) was at the level of pentaerythritol tetranitrate. The salts of 3-azido-4-(2H-tetrazol-5-yl)furazan with ammonia and guanylurea were also obtained and characterized. More... »

PAGES

779-785

References to SciGraph publications

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  • 2010-09-25. Theoretical studies on nitrogen rich energetic azoles in JOURNAL OF MOLECULAR MODELING
  • 2015-04. A new preparative method and some chemical properties of 4-R-furazan-3-carboxylic acid amidrazones in CHEMISTRY OF HETEROCYCLIC COMPOUNDS
  • 1984-09. Aminofurazans (review) in CHEMISTRY OF HETEROCYCLIC COMPOUNDS
  • 1994-05. Synthesis and properties of 4-amino-3-cyanofurazan in CHEMISTRY OF HETEROCYCLIC COMPOUNDS
  • 1993-11. Synthesis and reactivity of furazanyl- and furoxanyldiazonium salts in RUSSIAN CHEMICAL BULLETIN
  • 1994-04. Ring formation reactions of 4-aminofurazan-3-carboxyamidoximfs in CHEMISTRY OF HETEROCYCLIC COMPOUNDS
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    http://scigraph.springernature.com/pub.10.1007/s10593-017-2123-8

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    http://dx.doi.org/10.1007/s10593-017-2123-8

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