Reaction of 7-phenyl-7H-pyrazolo-[3,4-d][1,2,3]triazin-4-ol with thionyl chloride View Full Text


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Article Info

DATE

2013-09-10

AUTHORS

B. M. Khutova, S. V. Klyuchko, A. O. Gurenko, A. N. Vasilenko, E. B. Rusanov, V. S. Brovarets

ABSTRACT

The reaction of 7-phenyl-7H-pyrazolo[3,4-d][1,2,3]triazin-4-ol with thionyl chloride has been studied in the presence and absence of dimethyl formamide. It was found that heating the compound with thionyl chloride in the absence of dimethyl formamide gave 5-amino-1-phenyl-1H-pyrazole-4-carboxylic acid chloride and in its presence a mixture of 5-chloro-N-formyl-1-phenyl-1H-pyrazole-4-carboxamide, 5-chloro-1-phenyl-1H-pyrazole-4-carboxamide, and 4-chloro-6-(5-chloro-1-phenyl-1H-pyrazol-4-yl)-1-phenyl-1H-pyrazolo[3,4-d]pyrimidine.

PAGES

922-929

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10593-013-1327-9

DOI

http://dx.doi.org/10.1007/s10593-013-1327-9

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1010511711


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