Synthesis and aminomethylation of 9-aza-3-azoniaspiro[5,5]undeca-7,10-diene-8-selenolates View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-06

AUTHORS

K. A. Frolov, V. V. Dotsenko, S. G. Krivokolysko, R. I. Zubatyuk, O. V. Shishkin

ABSTRACT

10-Amino-7,11-dicyano-9-aza-3-azoniaspiro[5,5]undeca-7,10-diene-8-selenolates have been obtained by the interaction of N-alkylpiperidin-4-ones with 2 equiv. cyanoselenoacetamide or with malononitrile and cyanoselenoacetamide. Aminomethylation of the obtained compounds proceeded under mild conditions and led to the formation of 8'-selenoxo-3',5',7',11'-tetraazaspiro[piperidine-4,13'-tri-cyclo[7.3.1.02,7]tridec[2]ene]-1',9'-dicarbonitriles. The structure of 1-methyl-5',11'-di(4-methyl-phenyl)-8'-selenoxo-3',5',7',11'-tetraazaspiro[piperidine-4,13'-tricyclo[7.3.1.02,7]tridec[2]ene]-1',9'-di-carbonitrile was determined by X-ray structural analysis.

PAGES

472-478

References to SciGraph publications

  • 2009-02. Cascade synthesis of pyrimido-[4,3-b][1,3,5] selenadiazine derivatives in CHEMISTRY OF HETEROCYCLIC COMPOUNDS
  • 2007-01. An Efficient Mannich-Type One-Pot Synthesis of 3,5,7,11-Tetraazatricyclo [7.3.1.02,7]tridec-2-ene Derivatives Starting from Functionalized 1,4-Dihydropyridines in MONATSHEFTE FÜR CHEMIE - CHEMICAL MONTHLY
  • 2009. New Trends in Chemistry and Application of Aromatic and Related Selenaheterocycles in AROMATICITY IN HETEROCYCLIC COMPOUNDS
  • 2005. Thio-, Seleno-, Telluro-Amides in CHALCOGENOCARBOXYLIC ACID DERIVATIVES
  • 2000-03-22. Selenocarbonyls in ORGANOSELENIUM CHEMISTRY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/s10593-013-1270-9

    DOI

    http://dx.doi.org/10.1007/s10593-013-1270-9

    DIMENSIONS

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