Synthesis, molecular and crystal structure, and features of the electronic structure of bis(O’i)-chelated bis(2,2-dimethylbenzo-[2H]-4-oxo-1,3-oxazino-3-methyl)difluorosilane View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2006-12

AUTHORS

A. A. Korlyukov, K. A. Lysenko, M. Yu. Antipin, A. G. Shipov, E. P. Kramarova, T. P. Murasheva, Vad. V. Negrebetskii, Yu. E. Ovchinnikov, S. A. Pogozhikh, I. P. Yakovlev, Yu. I. Baukov

ABSTRACT

A method has been developed for the synthesis of a bis(O→Si)-chelated bis(2,2-dimethylbenzo[2H]-4-oxo-1,3-oxazino-3-methyl)difluorosilane from 2,2-dimethyl-3-trimethylsilylbenzo[2H]-1,3-oxazin-4-one and bis(chloromethyl)dichlorosilane via the intermediate formation of the corresponding unstable bis-chelated dichloride, subsequent hydrolysis with NaHCO3 and, without separation, treatment of the hydrolysis product with boron trifluoride etherate. Analysis of the electron density distribution showed the presence of dative bonding in both O→Si-F fragments. More... »

PAGES

1592-1602

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10593-006-0283-z

DOI

http://dx.doi.org/10.1007/s10593-006-0283-z

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1033154029


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