The mechanism of alkyl ketene dimer (AKD) sizing on cellulose model films studied by sum frequency generation vibrational spectroscopy View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2019-03

AUTHORS

Lei Li, David J. Neivandt

ABSTRACT

Sum frequency generation vibrational spectroscopy (SFS) was employed to study the alkyl ketene dimer (AKD) sizing mechanism employed in the papermaking industry for hydrophobization of cellulose. The AKD was spun coat onto model cellulose films, which resulted in ≈ 2.6 nm thick AKD layers. The chain orientation of AKD molecules during the sizing process was measured at different temperatures. It was demonstrated that the chain orientation and conformation of AKD do not correlate with observed changes in sizing. The distribution of AKD molecules on model cellulose surfaces as a function of time and temperature was imaged via fluorescence microscopy to complement SFS measurements. It was concluded that the distribution of AKD plays a major role in the sizing effect. More... »

PAGES

1-21

Journal

TITLE

Cellulose

ISSUE

5

VOLUME

26

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10570-019-02295-2

DOI

http://dx.doi.org/10.1007/s10570-019-02295-2

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1112141654


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