Surface functionalization of nanofibrillated cellulose using click-chemistry approach in aqueous media View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2011-10

AUTHORS

Nikolaos Pahimanolis, Ulla Hippi, Leena-Sisko Johansson, Tapio Saarinen, Nikolay Houbenov, Janne Ruokolainen, Jukka Seppälä

ABSTRACT

In the present work, amino functionalized nanofibrillated cellulose (NFC) was prepared using click-chemistry in aqueous reaction conditions. First, reactive azide groups were introduced on the surface of NFC by the etherification of 1-azido-2,3-epoxypropane in alkaline water/isopropanol-mixture at ambient temperature. Then the azide groups were reacted with propargyl amine utilizing copper catalyzed azide-alkyne cycloaddition (CuAAC), leading to pH-responsive 1,2,3-triazole-4-methanamine decorated NFC. The reaction products were characterized using Fourier transform infrared spectroscopy, elemental analysis and X-ray photoelectron spectroscopy. The presence of the attached azide groups was also confirmed by reacting them with 5-(dimethylamino)-N-(2-propyl)-1-naphthalenesulfonamide by CuAAC, yielding highly fluorescent NFC. In addition, atom force microscopy and rheology studies confirmed that the original NFC nanostructure was maintained during the synthesis. More... »

PAGES

1201

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10570-011-9573-4

DOI

http://dx.doi.org/10.1007/s10570-011-9573-4

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1012322891


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