Synthesis of Water-Dispersible Pd Nanoparticles Using a Novel Oxacalixarene Derivative and their Catalytic Application in C–C Coupling Reactions View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2016-08

AUTHORS

Viren Mehta, Manthan Panchal, Anita Kongor, Urvi Panchal, V. K. Jain

ABSTRACT

A novel 5,17-di(hydrazinecarbonyl) tetranitrooxacalix[4]arene (DHOC) derivative has been synthesized and characterized using various spectroscopic techniques. This DHOC derivative has been used to produce water-dispersible catalytically active Pd nanoparticles (PdNps). In the nanoparticle synthesis, DHOC serves as both a reducing and a stabilizing agent, thus simplifying the preparation of the PdNps because no separate reagents are required to reduce and stabilize the nanoparticles. These PdNps were characterized by a number of techniques such as Transmission Electron Microscopy and UV–Visible spectroscopy. The water-dispersible PdNps were 5 ± 2 nm in size and showed high catalytic activity in numerous C–C coupling reactions such as the Sonogashira, Suzuki-Miyuara and Heck reactions. More... »

PAGES

1581-1590

Journal

TITLE

Catalysis Letters

ISSUE

8

VOLUME

146

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10562-016-1781-y

DOI

http://dx.doi.org/10.1007/s10562-016-1781-y

DIMENSIONS

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44 schema:description A novel 5,17-di(hydrazinecarbonyl) tetranitrooxacalix[4]arene (DHOC) derivative has been synthesized and characterized using various spectroscopic techniques. This DHOC derivative has been used to produce water-dispersible catalytically active Pd nanoparticles (PdNps). In the nanoparticle synthesis, DHOC serves as both a reducing and a stabilizing agent, thus simplifying the preparation of the PdNps because no separate reagents are required to reduce and stabilize the nanoparticles. These PdNps were characterized by a number of techniques such as Transmission Electron Microscopy and UV–Visible spectroscopy. The water-dispersible PdNps were 5 ± 2 nm in size and showed high catalytic activity in numerous C–C coupling reactions such as the Sonogashira, Suzuki-Miyuara and Heck reactions.
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