One-Step Synthesis of a High Performance Pt-Fe3O4 Catalyst: Intermetallic Al13Fe4 as a Platform and Precursor View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2016-07

AUTHORS

Satoshi Kameoka, Satoru Wakabayashi, Eiji Abe, An Pang Tsai

ABSTRACT

A one-step process was developed to prepare catalysts with monodispersed Pt nanocrystals on Fe3O4, based on leaching of the intermetallic compounds Al76.5−xFe23.5Ptx (at%: x = 0, 0.05, 0.5, 1) with an aqueous 10 wt% NaOH solution. In this process, the intermetallic Al13Fe4 lattice acts as a platform in which Pt atoms can be homogeneously dispersed, and also serves as a precursor for subsequent leaching. Compared with conventional preparation methods, including impregnation and coprecipitation, this one-step process eliminates the need for thermal treatments such as high temperature calcination and/or reduction, thus minimizing the sintering or crystal grain growth problems caused by these treatments. Consequently, the materials derived from Al76Fe23.5Pt0.5 exhibit high catalytic performance during CO oxidation and the CO-PROX reaction due to the monodispersed Pt nanocrystals in the porous or nanoparticle Fe3O4 matrix. A high performance nanocomposite Pt-Fe3O4 catalyst, consisting of monodispersed Pt nanocrystals in a porous Fe3O4 matrix, was prepared by a one-step process based on caustic leaching of a bulk Al13(Fe + Pt)4 intermetallic compound. More... »

PAGES

1309-1316

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10562-016-1757-y

DOI

http://dx.doi.org/10.1007/s10562-016-1757-y

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