Polymerization on CO-Reduced Phillips Catalyst initiates through the C–H bond Activation of Ethylene on Cr–O Sites View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2014-05

AUTHORS

Murielle F. Delley, Matthew P. Conley, Christophe Copéret

ABSTRACT

Investigation of the polymerization of ethylene on CO-reduced Phillips catalyst (1 wt% chromium) by infrared spectroscopy reveals the presence of new OH bands. In particular, an OH-band appears at 3,605 cm−1, consistent with the interaction of the SiOH group with an adjacent Lewis acidic chromium center, Si–(μ-OH)–Cr. Polymerization with d4-ethylene leads to the formation of the isotopically shifted band at 2,580 cm−1, consistent with heterolytic C–H activation of ethylene over a Cr–O bond to generate the first Cr–C bond in ethylene polymerization with Phillips catalyst, as recently observed on well-defined Cr(III) silicates. More... »

PAGES

805-808

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10562-014-1238-0

DOI

http://dx.doi.org/10.1007/s10562-014-1238-0

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1003017872


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