Preparation of Silica-Based Ionic Liquid an Efficient and Recyclable Catalyst for One-Pot Synthesis of α-Aminonitriles View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2011-11

AUTHORS

Maryam Nouri Sefat, Dariush Saberi, Khodabakhsh Niknam

ABSTRACT

Preparation of N-(3-silicapropyl) imidazolium hydrogen sulfate ([Sipim]HSO4) as a heterogeneous acidic ionic liquid is described. This heterogeneous ionic liquid was used as catalyst for the synthesis of α-aminonitriles by a one-pot condensation of aldehydes, amines, and trimethylsilyl cyanide at room temperature. Catalyst could be recycled for several times without any additional treatment. A simple and efficient procedure for the preparation of silica-based acidic ionic liquid ([Sipim]HSO4) is described. This heterogeneous solid acid is employed as a catalyst for the synthesis of a-amino nitriles at room temperature. More... »

PAGES

1713

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URI

http://scigraph.springernature.com/pub.10.1007/s10562-011-0696-x

DOI

http://dx.doi.org/10.1007/s10562-011-0696-x

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https://app.dimensions.ai/details/publication/pub.1046089569


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