Effects of Sodium Acetate and Residual Aluminum on the Hydrogenation Rate, Optical Yield and Catalyst Durability for the Enantio-Differentiating Hydrogenation ... View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2009-03

AUTHORS

Shunli Cai, Kun Ma, Hangning Chen, Yunfeng Zheng, Jian Jiang, Rong Li

ABSTRACT

The effects of Na acetate and residual aluminum on the hydrogenation rate, optical yield and catalyst durability for the enantio-differentiating hydrogenation of methyl acetoacetate were studied over tartaric acid-modified Raney nickel catalysts with the in situ modification. There was an optimal Na acetate amount at which the highest optical yield and high hydrogenation rate were achieved. The addition of Na acetate in the repeat use could improve the catalyst durability significantly. The amount of the residual aluminum in Raney nickel catalysts also played an important role in this catalyst system. The highest optical yield of 61.6% was achieved over the improved T-1 RNi catalyst. Compared with previous literatures, this is the best result for the enantio-differentiating hydrogenation of methyl acetoacetate over in situ modified Raney nickel catalysts. More... »

PAGES

227-234

Journal

TITLE

Catalysis Letters

ISSUE

1-2

VOLUME

128

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10562-008-9742-8

DOI

http://dx.doi.org/10.1007/s10562-008-9742-8

DIMENSIONS

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