Preparation of Mesoporous V–Ce–Ti–O for the Selective Oxidation of Methanol to Dimethoxymethane View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2008-11

AUTHORS

Jingwei Liu, Qing Sun, Yuchuan Fu, Hongying Zhao, Aline Auroux, Jianyi Shen

ABSTRACT

Mesoporous V–Ce–Ti–O oxides were synthesized through the combination of sol–gel and hydrothermal methods and were characterized by different techniques. N2 adsorption showed that the mesoporous oxides with 0–20 wt.% V2O5 possessed the surface areas of about 160 m2 g−1 with narrow pore size distribution centered around 4–5 nm. Vanadium species were highly dispersed in the samples, as confirmed by the wide angle XRD and Raman spectroscopy. The surface acidity of the materials was determined by the microcalorimetric adsorption of NH3. Temperature programmed reduction and O2 chemisorption were used to probe the redox property of the materials. It was found that the mesoporous V–Ce–Ti–O possessed bifunctional characters of acidic and redox properties that catalyzed the oxidation of methanol to dimethoxymethane (DMM). These bifunctional characters were further enhanced by the addition of V2O5 and SO42− onto V–Ce–Ti–O simultaneously. Such supported catalysts exhibited excellent performance for the selective oxidation of methanol to DMM. Specifically, 72% conversion of methanol with 85% selectivity to DMM was achieved at 423 K over a SO42−–V2O5/V–Ce–Ti–O catalyst. More... »

PAGES

155-163

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10562-008-9598-y

DOI

http://dx.doi.org/10.1007/s10562-008-9598-y

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1026217187


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42 schema:description Mesoporous V–Ce–Ti–O oxides were synthesized through the combination of sol–gel and hydrothermal methods and were characterized by different techniques. N2 adsorption showed that the mesoporous oxides with 0–20 wt.% V2O5 possessed the surface areas of about 160 m2 g−1 with narrow pore size distribution centered around 4–5 nm. Vanadium species were highly dispersed in the samples, as confirmed by the wide angle XRD and Raman spectroscopy. The surface acidity of the materials was determined by the microcalorimetric adsorption of NH3. Temperature programmed reduction and O2 chemisorption were used to probe the redox property of the materials. It was found that the mesoporous V–Ce–Ti–O possessed bifunctional characters of acidic and redox properties that catalyzed the oxidation of methanol to dimethoxymethane (DMM). These bifunctional characters were further enhanced by the addition of V2O5 and SO42− onto V–Ce–Ti–O simultaneously. Such supported catalysts exhibited excellent performance for the selective oxidation of methanol to DMM. Specifically, 72% conversion of methanol with 85% selectivity to DMM was achieved at 423 K over a SO42−–V2O5/V–Ce–Ti–O catalyst.
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