A Chemical Potential Diagram and an In-situ X-ray Diffraction Analysis of a V–Mg–O Catalyst Used in the Oxidative Dehydrogenation of ... View Full Text


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Article Info

DATE

2009-01

AUTHORS

Norihito Kijima, Makoto Toba, Yuji Yoshimura

ABSTRACT

A chemical potential diagram of the V–Mg–O system was constructed for comparison in an in-situ experiment. A V–Mg–O catalyst used in the oxidative dehydrogenation of n-butane was prepared by the impregnation method and was characterized by in-situ X-ray diffraction (XRD). Mg3V2O8 and MgO were detected on the in-situ XRD pattern under the oxygen pretreatment at 600 °C, and the in-situ XRD data under working conditions showed that Mg3V2O8 is reduced to MgV2O4, having a cubic spinel structure with a lattice constant of a = 8.427 Å. The observed reduction of V5+ in Mg3V2O8 to V3+ in MgV2O4 under the working conditions could be well understood through a chemical potential diagram. More... »

PAGES

63

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10562-007-9353-9

DOI

http://dx.doi.org/10.1007/s10562-007-9353-9

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1051352199


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