X-ray scattering by nano-particles within granular thin films, investigation by grazing angle X-ray reflectometry View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

1999-02

AUTHORS

M. Mâaza, A. Gibaud, C. Sella, B. Pardo, F. Dunsteter, J. Corno, F. Bridou, G. Vignaud, A. Désert, A. Menelle

ABSTRACT

It is shown here that the observation of the phenomenon of like small angle scattering of X-rays in very thin heterogeneous films, can be made comparatively easily by using grazing angle reflectometry of X-rays. The feasibility was achieved with co-sputtered thin films of approximately 600 Å thickness, made up by crystalline platinum clusters embedded in an amorphous alumina matrix. The experimental reflectivity profiles are simulated by the intensity superposition of two components: (i) the specular part caused by the usual interference phenomenon between the partial waves reflected from the air-film and film-substrate interfaces, and (ii) the like-small angle scattering part due to diffraction by platinum clusters. It is found that the shape of such clusters is spherical characterized by mean values of diameter \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}\end{document} and inter-cluster distance \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}\end{document} of the order 29 Å and 45 Å respectively with standard deviations \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}\end{document} and \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}\end{document} of the order of 3 Å. Such an observation of both the interference and diffraction phenomena indicates that the thin granular film exhibits both its continuous and heterogeneous aspects together. More... »

PAGES

339-345

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s100510050620

DOI

http://dx.doi.org/10.1007/s100510050620

DIMENSIONS

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128 https://www.grid.ac/institutes/grid.462524.3 schema:alternateName Irradiated Solids Laboratory
129 schema:name Laboratoire des Solides Irradiés, École Polytechnique, Palaiseau, France, FR
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131 https://www.grid.ac/institutes/grid.462844.8 schema:alternateName Sorbonne University
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134 https://www.grid.ac/institutes/grid.5842.b schema:alternateName University of Paris-Sud
135 schema:name Institut d'Optique Théorique & Appliquée, Bâtiment 503, Université Paris-Sud, 91403 Orsay Cedex, France, FR
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