Electrochemical properties of spinel Li4Ti5O12 nanoparticles prepared via a low-temperature solid route View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2016-06-06

AUTHORS

Mamoru Senna, Martin Fabián, Ladislav Kavan, Markéta Zukalová, Jaroslav Briančin, Erika Turianicová, Patrick Bottke, Martin Wilkening, Vladimír Šepelák

ABSTRACT

Spinel phase Li4Ti5O12 (s-LTO) with an average primary particle size of 150 nm was synthesised via a solid state route by calcining a precursor mixture at 600 °C. The precursor was prepared from a stoichiometric mixture of TiO2 nanoparticles and an ethanolic solution of Li acetate and activated by ball-milling. Effects of the calcination temperature and atmosphere are examined in relation to the coexistence of impurity phases by X-ray diffraction and 6Li MAS NMR. The charge capacity of s-LTO, determined from cyclic voltammogram at a scan rate of 0.1 mV/s, was 142 mAh/g. The capacity of our optimised material is superior to that of commercially available spinel (a-LTO), despite the considerably smaller BET-specific surface area of the former. The superior properties of our material were also demonstrated by galvanostatic charging/discharging. From these observations, we conclude that the presented low-temperature solid state synthesis route provides LTO with improved electrochemical performance. More... »

PAGES

2673-2683

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10008-016-3272-x

DOI

http://dx.doi.org/10.1007/s10008-016-3272-x

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https://app.dimensions.ai/details/publication/pub.1016931569


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