Exploration of electrodeposited platinum alloy catalysts for methanol electro-oxidation in 0.5 M H2SO4: Pt-Ni system View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2004-11

AUTHORS

J. Mathiyarasu, A. M. Remona, A. Mani, K. L. N. Phani, V. Yegnaraman

ABSTRACT

In this work, we examine the electrocatalytic activity of electrodeposited Platinum (Pt)-Nickel (Ni) alloy layers on an inert substrate electrode for methanol oxidation reaction. Analyses using energy-dispersive fluorescent X-ray analysis and powder X-ray diffractometry confirm alloying of Pt with Ni in a range of compositions. Steady-state polarisation measurements in 0.5 M methanol+0.5 M H2SO4 solutions clearly show that the onset of electro-oxidation shifts to less anodic potential values (approximately 160 mV), while also exhibiting current enhancements up to ~15 times the currents obtained for the pure Pt electrodeposit. A linear relationship between the cyclic voltammetric peak (oxidation) current and [MeOH] is observed at a scan rate of 50 mVs−1, thus indicating reduced influence of adsorbed CO (COads) surface poison. A critical composition, Pt (92%)/Ni (8%) [denoted Pt-Ni(3) alloy] is found to exhibit maximum electrocatalytic activity, beyond which the activity drops, whereas pure Ni does not catalyse the reaction. While the promotion of electro-oxidation is understood to be largely due to the alloy catalyst, surface redox species of Ni oxide formed during the electro-oxidation process may also contribute to the oxygenation of COads, thereby enhancing the oxidation current. Plausible mechanisms of methanol oxidation on Pt/ transition metal alloy electrocatalysts are discussed in terms of electron transfer (in the alloy) and the role of Ni oxide species. More... »

PAGES

968-975

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s10008-004-0526-9

DOI

http://dx.doi.org/10.1007/s10008-004-0526-9

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1052149263


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