Method validation for determination of amino acids in feed by UPLC View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2017-10

AUTHORS

Katarzyna Szkudzińska, Ilona Smutniak, Jolanta Rubaj, Waldemar Korol, Grażyna Bielecka

ABSTRACT

The paper presents results of validation of an analytical procedure based on ultra-performance liquid chromatography technique (UPLC) for determination of 17 amino acids in different feeds. The following performance characteristics were determined for the investigated feeds: relative standard deviations of repeatability and intermediate precisions ranged from 0.4 % to 4.6 %, and from 0.8 % to 7.9 %, respectively; recovery rates ranged from 87 % to 104 %, and limit of detection was from 0.06 g kg−1 (methionine) to 0.72 g kg−1 (glutamic acid). Two approaches were used to estimate measurement uncertainty giving values in a range of 5.1 % to 5.5 %. These performance characteristics are in agreement with the values reported in Commission Regulation (EU) No 152/2009 for the ion exchange chromatography with spectrophotometric detection. More... »

PAGES

247-252

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s00769-017-1281-9

DOI

http://dx.doi.org/10.1007/s00769-017-1281-9

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1090937492


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