Microwave-assisted reaction of glycosylamine with aspartic acid View Full Text


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Article Info

DATE

2010-07

AUTHORS

Feliciana Real-Fernández, Francesca Nuti, M. Angeles Bonache, Marco Boccalini, Stefano Chimichi, Mario Chelli, Anna Maria Papini

ABSTRACT

The synthesis of N-protected glycosyl amino acids from amines has been investigated and it was found that, under microwave conditions, glycosylamines could be hydrolyzed leading to new products containing a glycosyl ester linkage. The efficiency of the microwave-induced glycosylation of aspartic acid was studied comparing the microwave activity between amide and ester bond formation. Different sugar moieties have been employed to demonstrate the simple and reproducible coupling methodology. New glycosyl ester compounds were further characterized by NMR spectroscopy. More... »

PAGES

599-604

References to SciGraph publications

  • 2006-01. The impact of microwave synthesis on drug discovery in NATURE REVIEWS DRUG DISCOVERY
  • 1994-04. A general approach to the synthesis ofO- andN-linked glycopeptides in GLYCOCONJUGATE JOURNAL
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/s00726-010-0484-8

    DOI

    http://dx.doi.org/10.1007/s00726-010-0484-8

    DIMENSIONS

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    PUBMED

    https://www.ncbi.nlm.nih.gov/pubmed/20130939


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