Single Ion Anisotropy of CrIII and FeIII in a Series of {Ti7M} Rings View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2020-10-30

AUTHORS

Andreas K. Kostopoulos, Grigore A. Timco, Floriana Tuna, Iñigo J. Vitórica-Yrezábal, George F. S. Whitehead, Heiko Bamberger, Joris van Slageren, David Collison, Eric J. L. McInnes, Richard E. P. Winpenny

ABSTRACT

A series of heterometallic [TiIV7MIII] rings are reported which contain a single paramagnetic metal centre, either FeIII or CrIII. The structures contain an octagon of metals bridged by oxides within the ring and pivalate ligands outside the ring. The structures encapsulate a single cation, either a secondary ammonium cation or a cesium. Multi-frequency EPR spectroscopy was used to measure the zero-field splitting parameters for the paramagnetic metal sites. The FeIII sites have rhombic anisotropy, with D around − 0.18 cm−1 and λ (= D/E) approximately 0.25. The CrIII have a more axial anisotropy, with D around − 0.5 cm−1 and λ around 0.05. Attempts to find a magneto-structural correlation are vitiated by the difficulty of refining the challenging crystal structures. More... »

PAGES

1251-1265

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s00723-020-01285-z

DOI

http://dx.doi.org/10.1007/s00723-020-01285-z

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1132144815


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