Improved Stability and Spectral Quality in Ex Situ Dissolution DNP Using an Improved Transfer Device View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2015-05-23

AUTHORS

Sotirios Katsikis, Ildefonso Marin-Montesinos, Miquel Pons, Christian Ludwig, Ulrich L. Günther

ABSTRACT

Dissolution dynamic nuclear polarization (DNP) has become one of the predominant implementations for DNP. However, the technical implementation of transferring the sample from the polarizer to the nuclear magnetic resonance (NMR) system remains challenging. There is a need for additional technical optimizations in order to use dissolution DNP for biochemical and chemical applications. Here we show how a newly designed pressure dissolution kit considerably improves spectral quality and stability by enabling highly reliable and fast sample transfer to the NMR system. More... »

PAGES

723-729

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s00723-015-0680-5

DOI

http://dx.doi.org/10.1007/s00723-015-0680-5

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1041734490


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