Novel synthesis of 2H-1,5-benzoxathiepin-3(4H)-one and 5H-4,1-benzoxathiepin-3(2H)-one derivatives and chemical properties evaluation View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2015-10

AUTHORS

Taras M. Tarasiuk, Olena O. Shyshkina, Yulian M. Volovenko, Volodymyr V. Medviediev, Tetiana A. Volovnenko, Oleg V. Shishkin

ABSTRACT

New methods for the synthesis of 2H-1,5-benzoxathiepin-3(4H)-one and 5H-4,1-benzoxathiepin-3(2H)-one derivatives have been developed. Carbonyl group of 2H-1,5-benzoxathiepin-3(4H)-one has been protected by cyclic and acyclic ketals. Interaction of 2H-1,5-benzoxathiepin-3(4H)-one with NaBH4, hydroxylamine, hydrazines, and Br2 has been investigated. Strecker reaction has been carried out for the synthesis of corresponding α-amino acid. Combination of Horner–Wadsworth–Emmons and Michael reactions allowed to obtain derivatives of β-substituted carboxylic acid. Also, 2H-1,5-benzoxathiepin-3(4H)-one have been involved in Johnson–Corey–Chaykovsky reaction. More... »

PAGES

1733-1742

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s00706-015-1500-1

DOI

http://dx.doi.org/10.1007/s00706-015-1500-1

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1004894289


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