Preparation of silica-bonded N-propyltriethylenetetramine as a recyclable solid base catalyst for the synthesis of 4,4′-(arylmethylene)bis(1H-pyrazol-5-ols) View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-07

AUTHORS

Khodabakhsh Niknam, Maryam Sadeghi Habibabad, Abdollah Deris, Nasrin Aeinjamshid

ABSTRACT

Silica-bonded N-propyltriethylenetetramine was prepared via the reaction between 3-silicapropyl chloride and triethylenetetramine. This heterogeneous solid base was used as a catalyst for the synthesis of 4,4′-(arylmethylene)bis(1H-pyrazol-5-ols) by a one-pot condensation of aromatic aldehydes with 3-methyl-1-phenyl-5-pyrazolone in 72–93 % yields. The catalyst could be recycled several times without any additional treatment.

PAGES

987-992

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s00706-012-0910-6

DOI

http://dx.doi.org/10.1007/s00706-012-0910-6

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1051087142


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