Microwave Digestion of Thermoluminescent Aluminium-Oxide Powders and Determination of Trace Impurities by Inductively Coupled Plasma Optical Emission Spectroscopy View Full Text


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Article Info

DATE

2000-08

AUTHORS

Gábor Molnár, József Borossay, Zsuzsanna B. Varga, Mária Ballók, András Bartha

ABSTRACT

Five commercial and three laboratory prepared thermoluminescent aluminium-oxide powders as well as three reference samples were digested by a microwave digestion system and the impurities were determined by ICP-OES. The physico-chemical properties of the different samples were found to influence highly the decomposition efficiency. Optimized decompositi on parameters were determined for the samples with different physico-chemical properties (phase composition, grain size). The detection limits of the impurities of interest are presented, the analysis results for the aluminium- oxide dosimetric samples and the standards are given as well for Be, Ca, Ce, Cu, Fe, Cd, Mg, Mo, Na, Ni, Ti and Zn in the < 2–400 μg/g range. More... »

PAGES

193-197

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s006040070037

DOI

http://dx.doi.org/10.1007/s006040070037

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1004195641


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