Enzyme-free electrocatalytic sensing of hydrogen peroxide using a glassy carbon electrode modified with cobalt nanoparticle-decorated tungsten carbide View Full Text


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Article Info

DATE

2019-04

AUTHORS

Muthaiah Annalakshmi, Paramasivam Balasubramanian, Shen-Ming Chen, Tse-Wei Chen

ABSTRACT

An efficient non-enzymatic electrochemical sensor for hydrogen peroxide (H2O2) was constructed by modifying a glassy carbon electrode (GCE) with a nanocomposite prepared from cobalt nanoparticle (CoNP) and tungsten carbide (WC). The nanocomposite was prepared at low temperature through a simple technique. Its crystal structure, surface morphology and elemental composition were investigated via X-ray diffraction, transmission electron microscopy and X-ray photoelectron spectroscopy. The results showed the composite to be uniformly distributed and that the CoNP are well attached to the surface of the flake-like WC. Electrochemical studies show that the modified GCE has an improved electrocatalytic activity toward the reduction of H2O2. H2O2 can be selectively detected, best at a working voltage of -0.4 V (vs. Ag/AgCl), with a 6.3 nM detection limit over the wide linear range from 50 nM to 1.0 mM. This surpasses previously reported non-enzymatic H2O2 sensors. The sensor was successfully applied to the determination of H2O2 in contact lens solutions and in spiked serum samples. Graphical abstract Schematic presentation of a method for electrochemical sensing of hydrogen peroxide in real samples using cobalt nanoparticle decorated tungsten carbide (WCC) modified glassy carbon electrode (GCE). More... »

PAGES

265

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s00604-019-3377-x

DOI

http://dx.doi.org/10.1007/s00604-019-3377-x

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1113143930

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/30929084


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