Electrostatic assembly of gold nanoparticles on black phosphorus nanosheets for electrochemical aptasensing of patulin View Full Text


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Article Info

DATE

2019-04

AUTHORS

Jinqiong Xu, Xiujuan Qiao, Yuan Wang, Qinglin Sheng, Tianli Yue, Jianbin Zheng, Ming Zhou

ABSTRACT

An aptamer based impedimetric assay for the mycotoxin patulin (PAT) is described. A glassy carbon electrode (GCE) was modified with black phosphorus nanosheets (BP NSs) and modified with PAT aptamer by electrostatic attraction. Detection is based on the variations of electron transfer resistance at the modified electrode surface. This assay can detect PAT over a linear range that extends from 1.0 nM to 1.0 μM with a 0.3 nM detection limit. To improve the performance of the sensor, the BP NS-GCE was further modified with gold nanoparticles and then with thiolated PAT aptamer. This modified electrode, operated at an applied potential of 0.18 V (vs. Ag/AgCl), has a wider linear range (0.1 nM to 10.0 μM) and a lower detection limits (0.03 nM). Both assays were successfully applied to the analysis of (spiked) genuine food samples. Graphical abstract Black phosphorus nanosheets (BP NSs) were used to fabricate an aptamer based assay for patulin. To further improve the performance of the electrode, gold nanoparticles (AuNP) were placed on the surface of black phosphorus nanosheets (AuNP-BP NSs) by electrostatic attraction for patulin aptasensing. More... »

PAGES

238

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s00604-019-3339-3

DOI

http://dx.doi.org/10.1007/s00604-019-3339-3

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1112731627

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/30868260


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