Alginate capped and manganese doped ZnS quantum dots as a phosphorescent probe for time-resolved detection of copper(II) View Full Text


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Article Info

DATE

2019-01

AUTHORS

Wen-Sheng Zou, Ming-Yue Deng, Ya-Qin Wang, Xiaoli Zhao, Wei-Hua Li, Xian-Huai Huang

ABSTRACT

A method is described for the detection of Cu(II). It is based on the use of a room-temperature phosphorescent probe consisting of alginate-capped and manganese(II)-doped ZnS quantum dots. The carboxy groups at the surface of the probe strongly coordinate Cu(II) to form a complex. As a result, the 4T1-6A1 transition of the Mn(II) ions in the probe is quenched, and the long decay time (~2.1 ms in the unquenched state) is accordingly reduced. At excitation/emission wavelengths of 316/590 nm and a delay time of 0.1 ms, the probe shows a linear response in the 0.01 to 12 μM Cu(II) concentration range. The detection limit is 6.0 nM and the RSD is 3.2% (for n = 5). Graphical Abstract A two-step procedure is described to synthesize alginate capped manganese doped ZnS QDs. These coordinate with Cu(II) to form an absorbent complex and can be used as a phosphorescent probe for time-resolved detection of Cu(II). More... »

PAGES

41

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URI

http://scigraph.springernature.com/pub.10.1007/s00604-018-3165-z

DOI

http://dx.doi.org/10.1007/s00604-018-3165-z

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PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/30569376


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