Optimization of lipase-catalyzed glucose ester synthesis in ionic liquids View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2010-01

AUTHORS

Sung Ho Ha, Nguyen Minh Hiep, Sang Hyun Lee, Yoon-Mo Koo

ABSTRACT

Lipase-catalyzed esterification of glucose with fatty acids in ionic liquids (ILs) mixture was investigated by using supersaturated glucose solution. The effect of ILs mixture ratio, substrate ratio, lipase content, and temperature on the activity and stability of lipase was also studied. The highest yield of sugar ester was obtained in a mixture of 1-butyl-3-methylimidazolium trifluoromethanesulfonate ([Bmim][TfO]) and 1-methyl-3-octylimidazolium bis[(trifluoromethyl)-sulfonyl]amide ([Omim][Tf(2)N]) with a volume ratio of 9:1, while Novozym 435 (Candida antarctica type B lipase immobilized on acrylic resin) showed the optimal stability and activity in a mixture of [Bmim][TfO] and [Omim][Tf(2)N] with a 1:1 volume ratio. Reuse of lipase and ILs was successfully carried out at the optimized reaction conditions. After 5 times reuse of Novozym 435 and ILs, 78% of initial activity was remained. More... »

PAGES

63

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URI

http://scigraph.springernature.com/pub.10.1007/s00449-009-0363-4

DOI

http://dx.doi.org/10.1007/s00449-009-0363-4

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https://app.dimensions.ai/details/publication/pub.1013687068

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/19680693


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