Solvent induced phenomena in a dendronized linear polymer View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2013-12

AUTHORS

Anja Kroeger, Baozhong Zhang, Christine Rosenauer, A. Dieter Schlüter, Gerhard Wegner

ABSTRACT

The properties of a dendronized linear polymer (DP) in dilute solutions depending on solvent quality and temperature are described. The polymer has a contour length of Lc = 1,060 nm. The sample of the fourth generation (PG4) was analyzed in the thermodynamically good solvents dioxane, chloroform, and methanol. The wormlike macromolecule has a persistence length lp = 7 nm in dioxane and a cross-section radius determined by small angle X-ray scattering (SAXS) of Rc (SAXS) = 2.8 nm. The bulk density of PG4 determined by SAXS was compared with solution density. Evidence for substantial swelling of the cross-section was found. Toluene acts as a thermodynamically poor solvent (θ solvent). Above the θ temperature Tθ , a strong temperature dependence of the size and the Young's modulus E was observed. Following Odijk, E/kBT ∼1 was found. Below Tθ , a regime characterized by unswelling of the wormlike chains was observed. The results suggest that DPs can be described as soft colloid filaments, which are subject to commonly observed interactions in colloidal systems. A phase diagram indicates a regime below Tθ in which fluctuations of osmotic pressure inside the filaments result in periodic undulation of the chains. In summary, introducing a dense dendritic shell around the backbone converts conventional polymers into molecular colloids. Figureᅟ More... »

PAGES

2879-2892

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s00396-013-3007-9

DOI

http://dx.doi.org/10.1007/s00396-013-3007-9

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1010833781

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/24293794


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