Ontology type: schema:ScholarlyArticle Open Access: True
2013-12
AUTHORSAnja Kroeger, Baozhong Zhang, Christine Rosenauer, A. Dieter Schlüter, Gerhard Wegner
ABSTRACTThe properties of a dendronized linear polymer (DP) in dilute solutions depending on solvent quality and temperature are described. The polymer has a contour length of Lc = 1,060 nm. The sample of the fourth generation (PG4) was analyzed in the thermodynamically good solvents dioxane, chloroform, and methanol. The wormlike macromolecule has a persistence length lp = 7 nm in dioxane and a cross-section radius determined by small angle X-ray scattering (SAXS) of Rc (SAXS) = 2.8 nm. The bulk density of PG4 determined by SAXS was compared with solution density. Evidence for substantial swelling of the cross-section was found. Toluene acts as a thermodynamically poor solvent (θ solvent). Above the θ temperature Tθ , a strong temperature dependence of the size and the Young's modulus E was observed. Following Odijk, E/kBT ∼1 was found. Below Tθ , a regime characterized by unswelling of the wormlike chains was observed. The results suggest that DPs can be described as soft colloid filaments, which are subject to commonly observed interactions in colloidal systems. A phase diagram indicates a regime below Tθ in which fluctuations of osmotic pressure inside the filaments result in periodic undulation of the chains. In summary, introducing a dense dendritic shell around the backbone converts conventional polymers into molecular colloids. Figureᅟ More... »
PAGES2879-2892
http://scigraph.springernature.com/pub.10.1007/s00396-013-3007-9
DOIhttp://dx.doi.org/10.1007/s00396-013-3007-9
DIMENSIONShttps://app.dimensions.ai/details/publication/pub.1010833781
PUBMEDhttps://www.ncbi.nlm.nih.gov/pubmed/24293794
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"description": "The properties of a dendronized linear polymer (DP) in dilute solutions depending on solvent quality and temperature are described. The polymer has a contour length of Lc\u2009=\u20091,060\u00a0nm. The sample of the fourth generation (PG4) was analyzed in the thermodynamically good solvents dioxane, chloroform, and methanol. The wormlike macromolecule has a persistence length lp\u2009=\u20097\u00a0nm in dioxane and a cross-section radius determined by small angle X-ray scattering (SAXS) of Rc (SAXS)\u2009=\u20092.8\u00a0nm. The bulk density of PG4 determined by SAXS was compared with solution density. Evidence for substantial swelling of the cross-section was found. Toluene acts as a thermodynamically poor solvent (\u03b8 solvent). Above the \u03b8 temperature T\u03b8 , a strong temperature dependence of the size and the Young's modulus E was observed. Following Odijk, E/kBT \u223c1 was found. Below T\u03b8 , a regime characterized by unswelling of the wormlike chains was observed. The results suggest that DPs can be described as soft colloid filaments, which are subject to commonly observed interactions in colloidal systems. A phase diagram indicates a regime below T\u03b8 in which fluctuations of osmotic pressure inside the filaments result in periodic undulation of the chains. In summary, introducing a dense dendritic shell around the backbone converts conventional polymers into molecular colloids. Figure\u115f",
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"name": "Colloid and Polymer Science",
"type": "Periodical"
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"issueNumber": "12",
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"name": "Solvent induced phenomena in a dendronized linear polymer",
"pagination": "2879-2892",
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