The application of a cavity ring-down spectrometer to measurements of ambient ammonia using traceable primary standard gas mixtures View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2016-08

AUTHORS

Nicholas A. Martin, Valerio Ferracci, Nathan Cassidy, John A. Hoffnagle

ABSTRACT

A correction for the undesirable effects of direct and indirect cross-interference from water vapour on ammonia (NH3) measurements was developed using an optical laser sensor based on cavity ring-down spectroscopy. This correction relied on new measurements of the collisional broadening due to water vapour of two NH3 spectral lines in the near infra-red (6548.6 and 6548.8 cm−1), and on the development of novel stable primary standard gas mixtures (PSMs) of ammonia prepared by gravimetry in passivated gas cylinders at 100 μmol mol−1. The PSMs were diluted dynamically to provide calibration mixtures of dry and humidified ammonia atmospheres of known composition in the nmol mol−1 range and were employed as part of establishing a metrological traceability chain to improve the reliability and accuracy of ambient ammonia measurements. The successful implementation of this correction will allow the extension of this rapid on-line spectroscopic technique to exposure chamber validation tests under controlled conditions and ambient monitoring in the field. More... »

PAGES

219

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s00340-016-6486-9

DOI

http://dx.doi.org/10.1007/s00340-016-6486-9

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https://app.dimensions.ai/details/publication/pub.1009057534


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