Hardening of smooth pulsed laser deposited PMMA films by heating View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2010-03

AUTHORS

Britta Fuchs, Felix Schlenkrich, Susanne Seyffarth, Andreas Meschede, Robert Rotzoll, Philipp Vana, Peter Großmann, Klaus Mann, Hans-Ulrich Krebs

ABSTRACT

Smooth poly(methyl methacrylate) (PMMA) films without any droplets were pulsed laser deposited at a wavelength of 248 nm and a laser fluence of 125 mJ/cm2. After deposition at room temperature, the films possess low universal hardness of only 3 N/mm2. Thermal treatments up to 200°C, either during deposition or afterwards, lead to film hardening up to values of 200 N/mm2. Using a combination of complementary methods, two main mechanisms could be made responsible for this temperature induced hardening effect well above the glass transition temperature of 102°C. The first process is induced by the evaporation of chain fragments and low molecular mass material, which are present in the film due to the ablation process, leading to an increase of the average molecular mass and thus to hardening. The second mechanism can be seen in partial cross-linking of the polymer film as soon as chain scission occurs at higher temperatures and the mobility and reactivity of the polymer material is high enough. More... »

PAGES

711-715

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s00339-009-5525-3

DOI

http://dx.doi.org/10.1007/s00339-009-5525-3

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1003646793


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