Synthesis, characterization, and Ni(II) ion sorption properties of poly(styrene-co-divinylbenzene) functionalized with aminophosphonic acid groups View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-01

AUTHORS

Corneliu-Mircea Davidescu, Mihaela Ciopec, Adina Negrea, Adriana Popa, Lavinia Lupa, Ecaterina-Stela Dragan, Radu Ardelean, Gheorghe Ilia, Smaranda Iliescu

ABSTRACT

In this study, novel chelating resins containing aminophosphonic acid groups grafted on poly(styrene-co-divinylbenzene) (1 % or 15 % DVB) were obtained by “one-pot” reactions. The phosphorus contents were determined in order to calculate the degree of functionalization with pendant aminophosphonic acid groups. The fraction of repetitive units functionalized with aminophosphonic acid groups was determined by accepting the statistical structure of the repetitive unit of initial and final copolymer. These materials were characterized by FT-IR spectroscopy, EDX, and TGA. Adsorption properties of aminophosphonic acids grafted on poly(styrene-co-divinylbenzene) were examined for the removal of Ni(II) ions from aqueous solutions using the batch equilibrium procedure. By applying the kinetic models to the experimental data it was found that the adsorption of Ni(II) on the studied chelating resins is described by the pseudo-second-order kinetic model. For all the studied systems, Langmuir isotherm model provided an excellent fit of the equilibrium adsorption data. More... »

PAGES

277-291

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s00289-012-0801-3

DOI

http://dx.doi.org/10.1007/s00289-012-0801-3

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1050882779


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38 schema:description In this study, novel chelating resins containing aminophosphonic acid groups grafted on poly(styrene-co-divinylbenzene) (1 % or 15 % DVB) were obtained by “one-pot” reactions. The phosphorus contents were determined in order to calculate the degree of functionalization with pendant aminophosphonic acid groups. The fraction of repetitive units functionalized with aminophosphonic acid groups was determined by accepting the statistical structure of the repetitive unit of initial and final copolymer. These materials were characterized by FT-IR spectroscopy, EDX, and TGA. Adsorption properties of aminophosphonic acids grafted on poly(styrene-co-divinylbenzene) were examined for the removal of Ni(II) ions from aqueous solutions using the batch equilibrium procedure. By applying the kinetic models to the experimental data it was found that the adsorption of Ni(II) on the studied chelating resins is described by the pseudo-second-order kinetic model. For all the studied systems, Langmuir isotherm model provided an excellent fit of the equilibrium adsorption data.
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