SPE and MSPD as pre-separation techniques for HPLC of tetracyclines in meat, milk and cheese View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

1997-09

AUTHORS

E. Brandšteterová, Pavel Kubalec, L’udmila Bovanová, Peter Šimko, Alena Bednáriková, L’ubomira Macháčková

ABSTRACT

Solid phase extraction (SPE) and Matrix solid phase dispersion (MSPD) have been tested as pre-separation procedures for high-performance liquid chromatography (HPLC) determination of tetracycline antibiotics in milk, meat and cheese. The extraction recoveries ranged from 48% to 86% for SPE and from 89% to 93% for MSPD at concentration levels of the maximal residual limits (MRL) recommended by the European Union to be 100 ng/g for the tetracyclines oxytetracycline (OTC), tetracycline (TC) and chlortetracycline (CTC). The detection limits were 15 – 22 ng/g for SPE and 30 ng/g for MSPD. Following the relatively simple SPE procedure we used a Lichrosorb RP-18 column and a diode array detector for HPLC. Results dealing with analysis of tetracyclines HPLC in cheese are published for the first time. More... »

PAGES

311-315

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s002170050171

DOI

http://dx.doi.org/10.1007/s002170050171

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1041253114


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