Comparison between conventional and ultrasound accelerated Tessier sequential extraction schemes for metal fractionation in sewage sludge View Full Text


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Article Info

DATE

1999-04

AUTHORS

B. Pérez-Cid, I. Lavilla, C. Bendicho

ABSTRACT

Chemical sequential extraction for metal fractionation in sewage sludge using the Tessier method has been accelerated by ultrasound. The two sequential extraction schemes (conventional and ultrasound accelerated) were compared in terms of extraction efficiency, precision, treatment time and partitioning patterns of metals. Extractable contents of Cu, Cr, Ni, Pb and Zn were measured by flame atomic absorption spectrometry, and the analytical results obtained by the two procedures were statistically compared (P = 0.95). No significant differences were found in the two first fractions (i.e. exchangeable and carbonate-bound), however, in the third and fourth extracts (i.e. Fe-Mn oxides-bound and organic matter-bound) the extraction capability of the two methods differed significantly. More... »

PAGES

667-672

Journal

TITLE

Journal of Analytical Chemistry

ISSUE

7

VOLUME

363

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s002160051269

DOI

http://dx.doi.org/10.1007/s002160051269

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1016885371


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