A multi-analytical approach for the characterization of powders from the Pompeii archaeological site View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2011-10

AUTHORS

Carmen Canevali, Paolo Gentile, Marco Orlandi, Francesca Modugno, Jeannette Jacqueline Lucejko, Maria Perla Colombini, Laura Brambilla, Sara Goidanich, Chiara Riedo, Oscar Chiantore, Pietro Baraldi, Cecilia Baraldi, Maria Cristina Gamberini

ABSTRACT

Nine black powders found in Pompeii houses in three different types of bronze vessels (cylindrical theca atramentaria, unguentaries, and aryballoi) were characterized in order to assess a correspondence between the composition and the type of vessel and, possibly, to verify if these powders were inks or not. For the compositional characterization, a multi-analytical approach was adopted, which involved the use of scanning electron microscopy-energy dispersive X-ray, Fourier-transformed infrared spectroscopy, Raman, X-ray diffraction, electron paramagnetic resonance spectroscopy, thermogravimetric analysis, gas chromatography coupled with mass spectrometry (GC/MS), and pyrolysis GC/MS. Powders contained in cylindrical theca atramentaria form a homogeneous group, and their organic and inorganic compositions suggest that they were writing inks, while powders contained in unguentaries and aryballoi could have had several different uses, including writing inks and cosmetics. Furthermore, the composition profile of the powders found in cylindrical cases shows that, at 79 AD: , in Pompeii, carbon-based inks were still used for writing, and iron gall inks had not been introduced yet. More... »

PAGES

1801

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s00216-011-5216-8

DOI

http://dx.doi.org/10.1007/s00216-011-5216-8

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1006839358

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/21735063


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