Poly(dimethylsiloxane) microchip capillary electrophoresis with electrochemical detection for rapid measurement of acetaminophen and its hydrolysate View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2004-08

AUTHORS

F. Y. He, A. L. Liu, X. H. Xia

ABSTRACT

Poly(dimethylsiloxane) microchip capillary electrophoresis with amperometric detection has been used for rapid separation and determination of acetaminophen and its hydrolysate, i.e. p-aminophenol. A Pt ultramicroelectrode with a diameter of 10 microm positioned at the outlet of the separation channel was used as a working electrode for amperometric detection. Factors influencing separation and detection were investigated and optimized. Results show that acetaminophen and p-aminophenol can be well separated within 35 s with RSD-1 (approximately 0.1 fmol) at S/ N=3. This method has been successfully applied to the detection of traces of p-aminophenol in paracetamol tablets. More... »

PAGES

1062-1067

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/s00216-004-2680-4

DOI

http://dx.doi.org/10.1007/s00216-004-2680-4

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1009586061

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/15221194


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