DSC And X-Ray Diffraction Coupling View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

1998-03

AUTHORS

G. Keller, F. Lavigne, L. Forte, K. Andrieux, M. Dahim, C. Loisel, M. Ollivon, C. Bourgaux, P. Lesieur

ABSTRACT

A new technique, that allows simultaneous time-resolved synchrotron X-ray diffraction as a function of temperature (XRDT) and high sensitivity DSC to be carried out in the same apparatus, has been developed. Microcalorimetry and XRDT scans can be performed at any rate between 0.01 and 10°C min−1 with a 0.01°C temperature resolution in the temperature range, 30–130°C and at lower cooling rates but the same heating rates in the −30–+30°C range. The use of a single and very small sample (1 to 20 μl) contained in a thin glass capillary for both measurements and simultaneous data collection prevents any temperature shift between recordings and any possible difference in the thermal histories of the samples. More... »

PAGES

783-791

References to SciGraph publications

  • 1996-11. Investigation of the complex thermal behavior of fats in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 1996-11. Thermal transitions of cassava starch at intermediate water contents in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/bf03341455

    DOI

    http://dx.doi.org/10.1007/bf03341455

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1036297035


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