One-potN-alkylation of primary amines to secondary amines by gold clusters supported on porous coordination polymers View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2009-12

AUTHORS

Tamao Ishida, Noriko Kawakita, Tomoki Akita, Masatake Haruta

ABSTRACT

Gold clusters and nanoparticles were deposited on the three kinds of porous coordination polymers (PCP5), MOF-5, CPL-2, and AI-MIL53 by the solid grinding method. The size of Au particles depended on the kinds of PCPs and increased in the order of AI-MIL53 < CPL-2 < MOF-5. The mean diameter of Au particles supported on AI-MIL53 was estimated to be 1.6 nm by HAADFSTEM. Such small Au clusters on AI-MIL53 can catalyze one-pot synthesis of secondary amines from primary amines by sequential oxidation/hydrogenation owing to the remarkable improvement of hydrogenation efficiency of imine. Gold clusters deposited on AI-MIL53 can also promoteN-alkylation of amine with alcohol to form a secondary amine under N2 atmosphere without using O2 and H2. More... »

PAGES

267-274

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf03214948

DOI

http://dx.doi.org/10.1007/bf03214948

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1046924922


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