31P and1H powder ENDOR study of ozonide radicals in carbonated apatites, synthesized from aqueous solutions View Full Text


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Article Info

DATE

1996-01

AUTHORS

S. Van Doorslaer, P. Moens, F. Callens, P. Matthys, R. Verbeeck

ABSTRACT

An O3− defect in Na+ CO32− containing apatite powder has been investigated with ENDOR after X-irradiation. The powder, synthesized by a hydrolysis of octo-calciumphosphate (OCP) and Na2CO3 was dried at 25°C until constant weight was reached. At low temperatures, both31P and1H ENDOR spectra were recorded for different settings of the magnetic field (i.e., when the magnetic field is swept through the EPR O3− spectrum). The ENDOR powder spectra were thoroughly analyzed using computer simulations based on the “orientation selection principle”. Interactions with two types of protons and two types of31P nuclei could be resolved. In this way, a detailed model could be established for the O3− ion in the hydroxyapatite lattice. The defect is located between two successive vacant hydroxyl sites. The axis connecting the two outer oxygen atoms (gy-axis) of the O3− ion is found to be along the hexagonalc-axis of the lattice. The twofold axis of the defect ion (gz-axis) is parallel to theb-axis of the lattice. More... »

PAGES

87-102

References to SciGraph publications

  • 1978-12. Radiogenic free radicals as molecular probes in bone in CALCIFIED TISSUE RESEARCH
  • 1981-12. ESR of CO2− in X-irradiated tooth enamel and A-type carbonated apatite in CALCIFIED TISSUE INTERNATIONAL
  • 1994-02. EPR study of carbonate derived and ozonide radicals in carbonated apatites synthesized from aqueous solutions in APPLIED MAGNETIC RESONANCE
  • 1993-12-01. Spectrum Decomposition through Maximum Likelihood Common Factor Analysis of the EPR Spectra of Na+ Containing Carbonated Apatites Dried at 400°C in CALCIFIED TISSUE INTERNATIONAL
  • 1964-12. Crystal Structure of Hydroxyapatite in NATURE
  • 1991-04. The effect of carbonate content and drying temperature on the ESR-spectrum near g=2 of carbonated calciumapatites synthesized from aqueous media in CALCIFIED TISSUE INTERNATIONAL
  • 1978-12. Paramagnetic and crystallographic effects of low temperature ashing on human bone and tooth enamel in CALCIFIED TISSUE RESEARCH
  • 1987-09. The contribution of CO33− and CO2− to the ESR spectrum near g=2 of powdered human tooth enamel in CALCIFIED TISSUE INTERNATIONAL
  • 1981-12. 13C enriched carbonate apatites studied by ESR: Comparison with human tooth enamel apatites in CALCIFIED TISSUE INTERNATIONAL
  • 1993-05. ESR study of 13C-enriched carbonated calciumapatites precipitated from aqueous solutions in CALCIFIED TISSUE INTERNATIONAL
  • 1995-04. 1H and31P ENDOR of the isotropic CO2− signal atg=2.0007 in the EPR spectra of precipitated carbonated apatites in APPLIED MAGNETIC RESONANCE
  • 1979-12. Study of an asymmetric ESR signal in X-irradiated human tooth enamel in CALCIFIED TISSUE INTERNATIONAL
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/bf03163101

    DOI

    http://dx.doi.org/10.1007/bf03163101

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1051216706


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