Preparation of aluminosilicate precursor by mechanochemical method from gibbsite-fumed silica mixtures View Full Text


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Article Info

DATE

1998-06

AUTHORS

J Temuujin, T S Jadambaa, K Okada, K J D Mackenzie

ABSTRACT

Aluminosilicate (mullite) precursor was prepared by mechanochemical treatment of gibbsite and fumed silica mixtures. The effect of grinding on its structure and thermal behaviour was examined by27Al and29Si MAS NMR, XRD, DTA-TG and FTIR. Thermal treatment of this precursor led to the crystallization of mullite at about 1200°C via a spinel-phase.27Al and29Si MAS NMR spectroscopies show lowering of mullitization temperature, which is associated with increased homogeneity of the precursor. Mechanochemical treatment of gibbsite and fumed silica mixtures resulted in the formation of a more homogeneous aluminosilicate precursor. More... »

PAGES

185-187

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf02744967

DOI

http://dx.doi.org/10.1007/bf02744967

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1033474879


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