Device to establish drying conditions for protective coatings at elevated temperatures View Full Text


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Article Info

DATE

1959-07

AUTHORS

A. W. Schwab, H. M. Teeter, J. C. Cowan

ABSTRACT

An apparatus has been described for determining the drying time of protective coatings at elevated temperatures, and tests have been made with vinyl ether formulations. The device is essentially a miniature Sanderson drying-time meter constructed in an oven where temperatures up to 260°C. can be maintained. Tolerances were made on the order of 0.015 in. for gear clearances and bearing expansion. A special high-temperature grease is the lubricant. Turntables, which make one revolution every 15 min., permit simultaneous evaluation of three films. Reproducible results have been obtained, and uniform conditions apparently prevail throughout the oven. Coatings are prepared by the spinning disc method, and under controlled conditions the film thickness is approximately 0.15 mil. “Tack-free time” and “dryto-touch time” are determined by the usual method of removing sand from the disc. Discs were stamped from aluminum as well as black iron, and differences in drying times observed. Coatings on black iron dry faster than those on aluminum, and its is presumed that iron plays the role of an oxidation or polymerization catalyst. More... »

PAGES

275-277

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf02639994

DOI

http://dx.doi.org/10.1007/bf02639994

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1012707938


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