Chromatostrip analysis of fatty acid derivatives View Full Text


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Article Info

DATE

1961-11

AUTHORS

T. H. Applewhite, M. J. Diamond, L. A. Goldblatt

ABSTRACT

Chromatostrips provide a rapid and convenient method of examination of samples by spot tests and by ascending or descending chromatography. Ascending chromatography for the examination of mixtures is carried out on 12×140-mm. glass strips coated with 5% starch-bonded silicic acid, while descending chromatography is done on 12×200-mm. strips. The 5% starch-bonded silicic acid coatings are resistant to normal handling, may be marked with a soft lead pencil, and may be stored indefinitely for reference. Three detection systems are employed: fluorescent minerals for conjugated unsaturates, fluorescein-bromine for unsaturates, and 2′,7′-dichlorofluorescein for all types of compounds. Positive tests result in characteristic spots when observed under normal or ultraviolet illumination. This permits the classification of components, after separation on the chromatostrips, into the groupings of conjugated unsaturated, unsaturated (or easily brominated), and saturated compounds. More... »

PAGES

609-614

References to SciGraph publications

  • 1960-09. The preparation of polyunsaturated aliphatic aldehydesvia the acyloin condensation in JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY
  • 1960-08. Fractionation of fats, oils, and waxes on thin layers of silicic acid in JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY
  • 1960-08. Dünnschicht-Chromatographie von Aminosäuren in CELLULAR AND MOLECULAR LIFE SCIENCES
  • 1960-06. Trennung einiger Vitamine der B-Gruppe und des Vitamins C durch Dünnschichtchromatographie in THE SCIENCE OF NATURE
  • 1960-05. Glycerolysis of marine oils and the preparation of acetylated monoglycerides in JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY
  • 1960-12. Untersuchungen Über Quantitative Serumlipidbestimmungen Mit Der Dünnschichtchromatographie in JOURNAL OF MOLECULAR MEDICINE
  • 1960-11. Analysis of complex lipid mixtures by thin-layer chromatography and complementary methods in JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY
  • 1960-07. Vicinally unsaturated hydroxy acids in seed oils in JOURNAL OF THE AMERICAN OIL CHEMISTS' SOCIETY
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    http://scigraph.springernature.com/pub.10.1007/bf02633370

    DOI

    http://dx.doi.org/10.1007/bf02633370

    DIMENSIONS

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