Scintillation emanometric determination of radium-226 in waters using a new method of radium preconcentration View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

1980-03

AUTHORS

J. Sedláĉek, F. Šebesta, P. Beneš

ABSTRACT

A modified method of scintillation emanometry for radium determination is described which uses a simple and effective preconcentration of dissolved radium by coprecipitation with a ternary complex of calcium phosphomolybdate and polyethylene glycol. After dissolution of the voluminous precipitate in an alkaline solution of ethylenediamine-tetraacetic acid and deemanation of radon by a simplified procedure, the activity of radon is measured in a scintillation cell. The accuracy and precision of the method are very good as shown by determination of radium-226 in standard solutions and in natural water samples distributed by IAEA in the frame of interlaboratory comparison program. Easy construction of a simple scintillation cell is described, yielding cells with reproducible parameters and sufficient sensitivity for radium analysis in natural waters. More... »

PAGES

45-53

References to SciGraph publications

  • 1980-03. New type of sorbents based on polyethers and some hydrophobic anions in JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/bf02516833

    DOI

    http://dx.doi.org/10.1007/bf02516833

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1033065535


    Indexing Status Check whether this publication has been indexed by Scopus and Web Of Science using the SN Indexing Status Tool
    Incoming Citations Browse incoming citations for this publication using opencitations.net

    JSON-LD is the canonical representation for SciGraph data.

    TIP: You can open this SciGraph record using an external JSON-LD service: JSON-LD Playground Google SDTT

    [
      {
        "@context": "https://springernature.github.io/scigraph/jsonld/sgcontext.json", 
        "about": [
          {
            "id": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/03", 
            "inDefinedTermSet": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/", 
            "name": "Chemical Sciences", 
            "type": "DefinedTerm"
          }, 
          {
            "id": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/0301", 
            "inDefinedTermSet": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/", 
            "name": "Analytical Chemistry", 
            "type": "DefinedTerm"
          }
        ], 
        "author": [
          {
            "affiliation": {
              "alternateName": "Department of Nuclear Chemistry, Technical University of Prague, B\u0159ehov\u00e1 7, 115 19, Prague, Czechoslovakia", 
              "id": "http://www.grid.ac/institutes/grid.6652.7", 
              "name": [
                "Department of Nuclear Chemistry, Technical University of Prague, B\u0159ehov\u00e1 7, 115 19, Prague, Czechoslovakia"
              ], 
              "type": "Organization"
            }, 
            "familyName": "Sedl\u00e1\u0109ek", 
            "givenName": "J.", 
            "id": "sg:person.015332676363.43", 
            "sameAs": [
              "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.015332676363.43"
            ], 
            "type": "Person"
          }, 
          {
            "affiliation": {
              "alternateName": "Department of Nuclear Chemistry, Technical University of Prague, B\u0159ehov\u00e1 7, 115 19, Prague, Czechoslovakia", 
              "id": "http://www.grid.ac/institutes/grid.6652.7", 
              "name": [
                "Department of Nuclear Chemistry, Technical University of Prague, B\u0159ehov\u00e1 7, 115 19, Prague, Czechoslovakia"
              ], 
              "type": "Organization"
            }, 
            "familyName": "\u0160ebesta", 
            "givenName": "F.", 
            "id": "sg:person.014502716325.78", 
            "sameAs": [
              "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.014502716325.78"
            ], 
            "type": "Person"
          }, 
          {
            "affiliation": {
              "alternateName": "Department of Nuclear Chemistry, Technical University of Prague, B\u0159ehov\u00e1 7, 115 19, Prague, Czechoslovakia", 
              "id": "http://www.grid.ac/institutes/grid.6652.7", 
              "name": [
                "Department of Nuclear Chemistry, Technical University of Prague, B\u0159ehov\u00e1 7, 115 19, Prague, Czechoslovakia"
              ], 
              "type": "Organization"
            }, 
            "familyName": "Bene\u0161", 
            "givenName": "P.", 
            "id": "sg:person.01237712015.74", 
            "sameAs": [
              "https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.01237712015.74"
            ], 
            "type": "Person"
          }
        ], 
        "citation": [
          {
            "id": "sg:pub.10.1007/bf02516841", 
            "sameAs": [
              "https://app.dimensions.ai/details/publication/pub.1049929857", 
              "https://doi.org/10.1007/bf02516841"
            ], 
            "type": "CreativeWork"
          }
        ], 
        "datePublished": "1980-03", 
        "datePublishedReg": "1980-03-01", 
        "description": "A modified method of scintillation emanometry for radium determination is described which uses a simple and effective preconcentration of dissolved radium by coprecipitation with a ternary complex of calcium phosphomolybdate and polyethylene glycol. After dissolution of the voluminous precipitate in an alkaline solution of ethylenediamine-tetraacetic acid and deemanation of radon by a simplified procedure, the activity of radon is measured in a scintillation cell. The accuracy and precision of the method are very good as shown by determination of radium-226 in standard solutions and in natural water samples distributed by IAEA in the frame of interlaboratory comparison program. Easy construction of a simple scintillation cell is described, yielding cells with reproducible parameters and sufficient sensitivity for radium analysis in natural waters.", 
        "genre": "article", 
        "id": "sg:pub.10.1007/bf02516833", 
        "inLanguage": "en", 
        "isAccessibleForFree": false, 
        "isPartOf": [
          {
            "id": "sg:journal.1094634", 
            "issn": [
              "0236-5731", 
              "1588-2780"
            ], 
            "name": "Journal of Radioanalytical and Nuclear Chemistry", 
            "publisher": "Springer Nature", 
            "type": "Periodical"
          }, 
          {
            "issueNumber": "1", 
            "type": "PublicationIssue"
          }, 
          {
            "type": "PublicationVolume", 
            "volumeNumber": "59"
          }
        ], 
        "keywords": [
          "natural water samples", 
          "effective preconcentration", 
          "alkaline solution", 
          "natural waters", 
          "radium determination", 
          "water samples", 
          "radium analysis", 
          "voluminous precipitate", 
          "ethylenediamine-tetraacetic acid", 
          "standard solutions", 
          "polyethylene glycol", 
          "preconcentration", 
          "ternary complex", 
          "sufficient sensitivity", 
          "determination", 
          "water", 
          "phosphomolybdate", 
          "coprecipitation", 
          "activity of radon", 
          "solution", 
          "glycol", 
          "dissolution", 
          "complexes", 
          "modified method", 
          "simplified procedure", 
          "acid", 
          "new method", 
          "easy construction", 
          "method", 
          "precipitates", 
          "scintillation cell", 
          "samples", 
          "radium", 
          "precision", 
          "sensitivity", 
          "IAEA", 
          "parameters", 
          "activity", 
          "cells", 
          "analysis", 
          "procedure", 
          "reproducible parameters", 
          "Interlaboratory Comparison Program", 
          "construction", 
          "emanometry", 
          "radon", 
          "Comparison Program", 
          "accuracy", 
          "frame", 
          "program", 
          "scintillation emanometry", 
          "calcium phosphomolybdate", 
          "deemanation of radon", 
          "deemanation", 
          "simple scintillation cell", 
          "Scintillation emanometric determination", 
          "emanometric determination", 
          "radium preconcentration"
        ], 
        "name": "Scintillation emanometric determination of radium-226 in waters using a new method of radium preconcentration", 
        "pagination": "45-53", 
        "productId": [
          {
            "name": "dimensions_id", 
            "type": "PropertyValue", 
            "value": [
              "pub.1033065535"
            ]
          }, 
          {
            "name": "doi", 
            "type": "PropertyValue", 
            "value": [
              "10.1007/bf02516833"
            ]
          }
        ], 
        "sameAs": [
          "https://doi.org/10.1007/bf02516833", 
          "https://app.dimensions.ai/details/publication/pub.1033065535"
        ], 
        "sdDataset": "articles", 
        "sdDatePublished": "2021-11-01T17:55", 
        "sdLicense": "https://scigraph.springernature.com/explorer/license/", 
        "sdPublisher": {
          "name": "Springer Nature - SN SciGraph project", 
          "type": "Organization"
        }, 
        "sdSource": "s3://com-springernature-scigraph/baseset/20211101/entities/gbq_results/article/article_153.jsonl", 
        "type": "ScholarlyArticle", 
        "url": "https://doi.org/10.1007/bf02516833"
      }
    ]
     

    Download the RDF metadata as:  json-ld nt turtle xml License info

    HOW TO GET THIS DATA PROGRAMMATICALLY:

    JSON-LD is a popular format for linked data which is fully compatible with JSON.

    curl -H 'Accept: application/ld+json' 'https://scigraph.springernature.com/pub.10.1007/bf02516833'

    N-Triples is a line-based linked data format ideal for batch operations.

    curl -H 'Accept: application/n-triples' 'https://scigraph.springernature.com/pub.10.1007/bf02516833'

    Turtle is a human-readable linked data format.

    curl -H 'Accept: text/turtle' 'https://scigraph.springernature.com/pub.10.1007/bf02516833'

    RDF/XML is a standard XML format for linked data.

    curl -H 'Accept: application/rdf+xml' 'https://scigraph.springernature.com/pub.10.1007/bf02516833'


     

    This table displays all metadata directly associated to this object as RDF triples.

    134 TRIPLES      22 PREDICATES      85 URIs      76 LITERALS      6 BLANK NODES

    Subject Predicate Object
    1 sg:pub.10.1007/bf02516833 schema:about anzsrc-for:03
    2 anzsrc-for:0301
    3 schema:author N44db8625efa447bda5f33641698fe190
    4 schema:citation sg:pub.10.1007/bf02516841
    5 schema:datePublished 1980-03
    6 schema:datePublishedReg 1980-03-01
    7 schema:description A modified method of scintillation emanometry for radium determination is described which uses a simple and effective preconcentration of dissolved radium by coprecipitation with a ternary complex of calcium phosphomolybdate and polyethylene glycol. After dissolution of the voluminous precipitate in an alkaline solution of ethylenediamine-tetraacetic acid and deemanation of radon by a simplified procedure, the activity of radon is measured in a scintillation cell. The accuracy and precision of the method are very good as shown by determination of radium-226 in standard solutions and in natural water samples distributed by IAEA in the frame of interlaboratory comparison program. Easy construction of a simple scintillation cell is described, yielding cells with reproducible parameters and sufficient sensitivity for radium analysis in natural waters.
    8 schema:genre article
    9 schema:inLanguage en
    10 schema:isAccessibleForFree false
    11 schema:isPartOf N56ccf8c4f95c41c2be80db6f3c5365fc
    12 N8c6649e4492c4badbd0cef133522b8f9
    13 sg:journal.1094634
    14 schema:keywords Comparison Program
    15 IAEA
    16 Interlaboratory Comparison Program
    17 Scintillation emanometric determination
    18 accuracy
    19 acid
    20 activity
    21 activity of radon
    22 alkaline solution
    23 analysis
    24 calcium phosphomolybdate
    25 cells
    26 complexes
    27 construction
    28 coprecipitation
    29 deemanation
    30 deemanation of radon
    31 determination
    32 dissolution
    33 easy construction
    34 effective preconcentration
    35 emanometric determination
    36 emanometry
    37 ethylenediamine-tetraacetic acid
    38 frame
    39 glycol
    40 method
    41 modified method
    42 natural water samples
    43 natural waters
    44 new method
    45 parameters
    46 phosphomolybdate
    47 polyethylene glycol
    48 precipitates
    49 precision
    50 preconcentration
    51 procedure
    52 program
    53 radium
    54 radium analysis
    55 radium determination
    56 radium preconcentration
    57 radon
    58 reproducible parameters
    59 samples
    60 scintillation cell
    61 scintillation emanometry
    62 sensitivity
    63 simple scintillation cell
    64 simplified procedure
    65 solution
    66 standard solutions
    67 sufficient sensitivity
    68 ternary complex
    69 voluminous precipitate
    70 water
    71 water samples
    72 schema:name Scintillation emanometric determination of radium-226 in waters using a new method of radium preconcentration
    73 schema:pagination 45-53
    74 schema:productId N33048b6baa7b4a4081b4c19b29f145ee
    75 Nef8b08a2cef1436f81f11d60e2f7a203
    76 schema:sameAs https://app.dimensions.ai/details/publication/pub.1033065535
    77 https://doi.org/10.1007/bf02516833
    78 schema:sdDatePublished 2021-11-01T17:55
    79 schema:sdLicense https://scigraph.springernature.com/explorer/license/
    80 schema:sdPublisher N85c01e11a3ed45ab9459747fa1b2e599
    81 schema:url https://doi.org/10.1007/bf02516833
    82 sgo:license sg:explorer/license/
    83 sgo:sdDataset articles
    84 rdf:type schema:ScholarlyArticle
    85 N33048b6baa7b4a4081b4c19b29f145ee schema:name doi
    86 schema:value 10.1007/bf02516833
    87 rdf:type schema:PropertyValue
    88 N44db8625efa447bda5f33641698fe190 rdf:first sg:person.015332676363.43
    89 rdf:rest Ne592695c54a448c7898ca5ca73a08db6
    90 N56ccf8c4f95c41c2be80db6f3c5365fc schema:issueNumber 1
    91 rdf:type schema:PublicationIssue
    92 N7a3dab31710f42c9a77888bba3b94bd9 rdf:first sg:person.01237712015.74
    93 rdf:rest rdf:nil
    94 N85c01e11a3ed45ab9459747fa1b2e599 schema:name Springer Nature - SN SciGraph project
    95 rdf:type schema:Organization
    96 N8c6649e4492c4badbd0cef133522b8f9 schema:volumeNumber 59
    97 rdf:type schema:PublicationVolume
    98 Ne592695c54a448c7898ca5ca73a08db6 rdf:first sg:person.014502716325.78
    99 rdf:rest N7a3dab31710f42c9a77888bba3b94bd9
    100 Nef8b08a2cef1436f81f11d60e2f7a203 schema:name dimensions_id
    101 schema:value pub.1033065535
    102 rdf:type schema:PropertyValue
    103 anzsrc-for:03 schema:inDefinedTermSet anzsrc-for:
    104 schema:name Chemical Sciences
    105 rdf:type schema:DefinedTerm
    106 anzsrc-for:0301 schema:inDefinedTermSet anzsrc-for:
    107 schema:name Analytical Chemistry
    108 rdf:type schema:DefinedTerm
    109 sg:journal.1094634 schema:issn 0236-5731
    110 1588-2780
    111 schema:name Journal of Radioanalytical and Nuclear Chemistry
    112 schema:publisher Springer Nature
    113 rdf:type schema:Periodical
    114 sg:person.01237712015.74 schema:affiliation grid-institutes:grid.6652.7
    115 schema:familyName Beneš
    116 schema:givenName P.
    117 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.01237712015.74
    118 rdf:type schema:Person
    119 sg:person.014502716325.78 schema:affiliation grid-institutes:grid.6652.7
    120 schema:familyName Šebesta
    121 schema:givenName F.
    122 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.014502716325.78
    123 rdf:type schema:Person
    124 sg:person.015332676363.43 schema:affiliation grid-institutes:grid.6652.7
    125 schema:familyName Sedláĉek
    126 schema:givenName J.
    127 schema:sameAs https://app.dimensions.ai/discover/publication?and_facet_researcher=ur.015332676363.43
    128 rdf:type schema:Person
    129 sg:pub.10.1007/bf02516841 schema:sameAs https://app.dimensions.ai/details/publication/pub.1049929857
    130 https://doi.org/10.1007/bf02516841
    131 rdf:type schema:CreativeWork
    132 grid-institutes:grid.6652.7 schema:alternateName Department of Nuclear Chemistry, Technical University of Prague, Břehová 7, 115 19, Prague, Czechoslovakia
    133 schema:name Department of Nuclear Chemistry, Technical University of Prague, Břehová 7, 115 19, Prague, Czechoslovakia
    134 rdf:type schema:Organization
     




    Preview window. Press ESC to close (or click here)


    ...