Separation of technical waxes by temperature-programmed packed-capillary liquid chromatography View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2000-03

AUTHORS

P. Molander, E. Ommundsen, T. Greibrokk

ABSTRACT

A high-melting saturated hydrocarbon wax in the carbon range C28 to C90, with an average molecular mass of 785, and a saponified, oxidized Fisher-Tropsch wax of average molecular mass 745 have been characterized by reversed-phase packed-capillary liquid chromatography with isocratic nonaqueous mobile phases. High-temperature injection, temperature-programming, and miniaturized evaporative light-scattering detection were successfully employed for these separations. The injection of the wax samples, of low solubility at ambient temperature, was achieved by use of a high-temperature sample-introduction device. Temperature programming was required to achieve satisfactory resolution between the numerous components of the complex was samples. More... »

PAGES

349-352

References to SciGraph publications

Journal

TITLE

Chromatographia

ISSUE

5-6

VOLUME

51

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf02490615

DOI

http://dx.doi.org/10.1007/bf02490615

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1046131226


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