Determination of alkylphenols in water samples by solid-phase extraction on to poly(styrene-divinylbenzene) and quantification by liquid chromatography with UV-detection View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

1998-11

AUTHORS

A. M. Kvistad, E. Lundanes, T. Greibrokk

ABSTRACT

A method for determination of alkylphenols in water samples has been developed and validated. The alkylphenols were extracted on to polystyrene solid-phase columns. Six replicates could be processed in parallel in approximately 30 min using home-made equipment. Quantification was performed by reversed-phase liquid chromatography with UV-detection at 278 nm. The method has been validated for determination of 4-n-hexylphenol, 4-tert-octylphenol and nonylphenol in the concentration range 1–100 μg L−1 with 4-n-heptylphenol and/or 4-n-octylphenol as internal standard(s). The repeatability of the method was 1–6%RSD, and the intermediate precision was 1–3%RSD at the 100 μg L−1 level. The accuracy, determined as recovery, was 98–104%. The limit of detection (LOD) was 0.1–0.2 μg L−1 for 1-L water samples. The method has been used for determination of alkylphenols in samples of aquarium water. More... »

PAGES

707-713

Journal

TITLE

Chromatographia

ISSUE

9-10

VOLUME

48

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf02467603

DOI

http://dx.doi.org/10.1007/bf02467603

DIMENSIONS

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