Sn(II)-Treated MoO3 as cathode material for rechargeable lithium batteries View Full Text


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Article Info

DATE

2002-05

AUTHORS

A. M. Hashim, G. H. Wrodnigg, M. H. Askar, M. Winter, J. H. Albering, J. O. Besenhard

ABSTRACT

We report on the synthesis and structural, thermal and electrochemical characterisation of reduced molybdenum oxides with layered α-MoO3 type structure. The samples have been prepared by reactions of various amounts of water-free tin dichloride with fine-particulated orthorhombic molybdenum trioxide in n-hexane (non-aqueous media) or in aqueous media, which yielded materials with different Sn:Mo ratio. XRD investigations of these materials proved that the crystal structure of the layered α-MoO3 has been maintained after the reduction process. No crystalline impurity phases (e.g. tin oxides) could be detected by XRD. The tin-reduced samples exhibited a drastically improved cycling stability and capacity retention on cycling in 1 M LiClO4/propylene carbonate, i.e. the discharge capacities were well above 100 mAh g−1 after 20 cycles whereas the non-treated MoO3 (reference sample) has retained only about 45 mAh g−1. At higher cycle numbers (approx. cycle 100) the discharge capacity of the reduced molybdenum oxides stabilises at a level of approx. 100 mAh g−1. This significant improvement of the rechargeability may be related to improved electronic conductivity and/or higher structural stabilisation of the layered MoO3 structure either due to (i) a coating of the MoO3 particles with a protective thin layer of a tin containing compounds, and/or (ii) an amorphisation of the structure after reductive treatment. Further efforts of this study were devoted to a variation of the conductive carbon content in the electrode composition and to changes of cut-off voltages and current densities. More... »

PAGES

183-191

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URI

http://scigraph.springernature.com/pub.10.1007/bf02376067

DOI

http://dx.doi.org/10.1007/bf02376067

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https://app.dimensions.ai/details/publication/pub.1047811101


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