Directly coupled supercritical-fluid extraction/capillary supercritical-fluid chromatography of polymer additives View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

1991-12

AUTHORS

H. Daimon, Y. Hirata

ABSTRACT

The direct coupling of supercritical-fluid extraction (SFE) to capillary, supercritical-fluid chromatography (SFC) is described. The SFE/SFC system has a flame ionization detector and a direct injection system. The interface consists of a developed restrictor unit and a trapping tube. The fluid extract is decompressed through a restrictor into the trap where the solutes are precipitated and concentrated. The solutes are transferred from the trap to the capillary column by valve switching. The efficiency of various traps has been evaluated using n-paraffin standards. The effect of extraction temperature and pressure on the extraction efficiency is discussed for polymer additives. The applicability of the SFE/SFC system is demonstrated using several polypropylene samples. More... »

PAGES

549-554

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf02327902

DOI

http://dx.doi.org/10.1007/bf02327902

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1040826974


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