Preparation of [48V]-VO2+ for biomedical studies View Full Text


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Article Info

DATE

1995-07

AUTHORS

S. K. Zeisler, T. J. Ruth

ABSTRACT

A new method for the highly efficient separation of48V for radiotracer experiments is presented. It is based on the proton irradiation of a high purity Ti plate which is dissolved in sulfuric acid to form Ti3+ and V4+. Both ions are quantitatively absorbed on AG50W-X8 cation exchange resin and are converted to the respective higher valence state by an on-column reaction with diluted nitric acid and hydrogen peroxide. The eluate containing V5+ is evaporated to dryness in presence of sulfuric acid and treated with ethanol to reduce [48V]-vanadate to [48V]-vanadyl for labeling experiments in pharmaceutical research. More... »

PAGES

283-290

References to SciGraph publications

  • 1989-12. Vanadium transport across placenta and milk of rats to the fetus and newborn in BIOLOGICAL TRACE ELEMENT RESEARCH
  • 1994-08. A radiochemical method of separation of carrier-free vanadium from scandium and bulk amount of titanium in JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
  • 1989-12. Preparation of no-carrier-added48V(IV) and48V(V) for biological tracer use in JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/bf02163782

    DOI

    http://dx.doi.org/10.1007/bf02163782

    DIMENSIONS

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