Mössbauer study of internally oxidized silver-tin alloys View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

1984-11

AUTHORS

F. H. Sánchez, R. C. Mercader, A. F. Pasquevich, A. G. Bibiloni, A. López-García

ABSTRACT

A Mössbauer study of internally formed oxides as a function of oxidation temperatures between 200 ‡C and 850 ‡C was performed on previously annealed 1 at%AgSn alloys. The oxide formed at high temperatures (t ⩾ 500 ‡C) consists in agglomerates of tin dioxide = 0.00 ± 0.01 mm/s, δQ=0.50 ± 0.03 mm/s). The low temperature oxide (t ⩽ 300 ‡C) is characterized by = 0.29 ± 0.02 mm/s and δQ=0.32 ± 0.03 mm/s, and could be in the form of one-Sn-atom oxide complexes in the silver matrix. From the measured isomer shifts in the range 400 ⩽t ⩽ 550 ‡C, the maximum contribution of the silver matrix to the effective number of electrons per Sn atom in oxide agglomerates has been estimated ℴ have a value of about 0.06. The effect of the cold work on the hyperfine parameters of the oxidized tin has also been investigated. ‘As rolled ’ samples were found to attain the same values of isomer shifts and quadrupole splittings as annealed specimens, but at lower temperatures. More... »

PAGES

295-303

Journal

TITLE

Hyperfine Interactions

ISSUE

4

VOLUME

20

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf02069378

DOI

http://dx.doi.org/10.1007/bf02069378

DIMENSIONS

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